One embodiment relates to a method for the separation and recovery of a laminate that includes a step for immersing a laminate provided with at least a polyolefin base material layer and a release layer in contact with the polyolefin base material layer in a release solution containing a surfactant having an HLB value of 7 or more and a defoamer having an HLB value of 1-3, releasing the release layer, and recovering the polyolefin base material, the release layer being a layer including a water-soluble resin or a compound having an acidic group.

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